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Technical data


Haloalkanes: Grignard reagent

Article no: P3101000

Principle

Haloalkanes react with magnesium to the so-called Grignard reagents in accordance with the general formula RMgX. With X = bromide or iodide, the reaction works best. Chlorides are usually more inert and require higher temperatures and longer reaction times for the conversion. The compounds that were discovered by Victor Grignard probably exist as dimeric structures.

Benefits

  • Secure connection of the items by GL screw joint system
  • Stable and safe setup due to solid stand material

Tasks

Investigate the reaction of n-propyl bromide with magnesium turnings in tetrahydrofuran.

Learning objectives

  • n-propyl bromide
  • Magnesium
  • Haloalkanes
  • Grignard reagent
  • Organometallic compounds

Necessary accessories

  • Precision balance 620g/0.001g

Scope of delivery

Support base DEMO 02007-55 1
Stand rods, stainless steel, various sizes 02037-00 2
Retort stand, h = 750 mm 37694-00 1
Right angle boss-head clamp 37697-00 6
Universal clamp 37715-01 6
Three neck round bottom flask, 100 ml MAU-27220501 1
Round bottom flask, 100ml, GL 25/12 MAU-27100001 1
Dropping funnel, 50 ml, Gl 18 MAU-27222000 1
Funnel for gas generator, 50 ml, GL18 MAU-27222500 1
Dimroth-Condensor, GL 25/12 MAU-27223500 1
Gasket for GL25, 8mm hole, 10 pcs 41242-03 1
Calcium chloride tube,str.150 mm 36941-00 2
Stopcock,3-way,t-shaped, glass 36731-00 1
Gasometer 1000 ml 40461-00 1
Plastic bag w. hose 10 u. 40469-00 1
Pinchcock, width 15 mm 43631-15 1
Graduated cylinders, Boro, various sizes 36629-00 1
Magnetic stirrer without heating, 3 ltr., 230 V 35761-99 1
Magnetic stirring bar 15 mm, cylindrical 46299-01 1
Magnetic stirring bar 30 mm, cylindrical 46299-02 1
Magnetic stirring bar, 50 mm, cylindrical 46299-03 1
Separator for magnetic bars 35680-03 1
Lab thermometer,-10..+110 °C 38056-00 1
Weather monitor with big display 87997-10 1
Rubber hose, various diameters 39282-00 3
Hose clip, diam. 8-16 mm, 1 pc. 40996-02 2
Filtration stand for 2 funnels 33401-88 1
Funnels (glass), Boro, various sizes 34459-00 1
Round filters, 100 pcs., various sizes 32977-06 1
Powder funnels, plastic, various sizes 34472-00 1
Spoon, special steel 33398-00 1
Microspoon, steel 33393-00 1
Wash bottle, plastic, 500 ml 33931-00 1
Rubber stopper, d = 22/17 mm, 1 hole 39255-01 1
Glass wool 10 g 31773-03 1
Calcium chloride, granul. 250 g 48021-25 1
Tetrahydrofuran 1000 ml 31883-70 1
Potassium hydroxide pellets,500 g 30103-50 1
Magnesium,turnings,grignard 50 g 30134-05 1
Iodine resublimed 25 g 30093-04 1
Water, distilled 5 l 31246-81 1

PHYWE Systeme GmbH & Co. KG
Robert-Bosch-Breite 10 – 37079 Göttingen – Germany
www.phywe.com